“水质丁基黄原酸的测定液相色谱-三重四极杆串联质谱法”(HJ 1002-2018)的实验室方法验证

hinaР The determination（ of water quality-determination of butyl xanthate， - liquid chromatography/triple， ） quadrupoleР tandemAbstract mass： spectrometry HJ 1002-2018 was validated by determining the detection limit lower limit accuracy andР precision. The results showed（ that the detection） limit of butyl xanthate was 0.08 μg/L which was， less than，0.2 μg/L. TheР precision test of butyl xanthate at low middle and high concentrations 1.0 μg/L 10，.0 μg/L and 100 μg/L was carriedР out. The standard deviations were 4.6%， 0.7% and 0.9%. The recovery（ of butyl xanthate， in surface water is 97）%~103%Р and the accuracy and precision meet the， requirements of quality control. ，Р butyl xanthate HPLC-MS/MS method validationР Key words： ； ；