i/d4.835100.070.0318.3319.1650.10341.29932.9581.01.0830.18115.0910.16902.12372.52145.060.01135.57117.7860.19832.49162.4142.03.01237.21218.6060.20712.60262.09062.0100.01643.24221.6210.23923.00561.9186.011.01947.35223.6760.26073・27551.60820.042.02757.21328.6070.31083.90551.47733.075.03262.83331.4160.33844.25191.41211.026.03566.07333.0360.35394.44701.2744.011.04374.34437.1720.39224.92851.2602.05.04475.36337.6810.39684.98611.2067.020.04879.34439.6720.41445・20741.1705.014.05182.31541.1570.42725・36841.0884.012.05990.11445.0570.45945・77361.0443.010.06495.00547.5030.47866.01420.9653.010.075105.90652.9530.51816.51050.9581.04.076106.90653.4530.52156.55310.9345.018.080111.03655.5180.53516.72390.9172.07.083114.19757.0990.54506.8487六、实验结论通过MDIJade5物相检索,与标准PDF卡片对比,确认XRD所测物质为Li4Ti5012,且晶格常数为8.3588埃,符合实验。